Technology Process of C20H10Br2F2S2
There total 6 articles about C20H10Br2F2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; acetic acid / chloroform / 3 h / 50 °C
2: (1S)-10-camphorsulfonic acid; (tetrahydrothiophene)gold(III) bromide; (4-fluorophenyl)-λ3-iodanediyl diacetate / chloroform-d1; d(4)-methanol / 30 °C
With
N-Bromosuccinimide; (tetrahydrothiophene)gold(III) bromide; (4-fluorophenyl)-λ3-iodanediyl diacetate; (1S)-10-camphorsulfonic acid; acetic acid;
In
chloroform-d1; chloroform; d(4)-methanol;
DOI:10.1021/ja408712e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; potassium fluoride / tetrahydrofuran / 1 h / 20 °C / Schlenk technique; Inert atmosphere
2: N-Bromosuccinimide; acetic acid / chloroform / 3 h / 50 °C
3: (1S)-10-camphorsulfonic acid; (tetrahydrothiophene)gold(III) bromide; (4-fluorophenyl)-λ3-iodanediyl diacetate / chloroform-d1; d(4)-methanol / 30 °C
With
potassium fluoride; N-Bromosuccinimide; (tetrahydrothiophene)gold(III) bromide; (4-fluorophenyl)-λ3-iodanediyl diacetate; (1S)-10-camphorsulfonic acid; palladium diacetate; acetic acid;
In
tetrahydrofuran; chloroform-d1; chloroform; d(4)-methanol;
DOI:10.1021/ja408712e
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; acetic acid / chloroform / 3 h / 50 °C
2: (1S)-10-camphorsulfonic acid; (4-fluorophenyl)-λ3-iodanediyl diacetate; (triphenylphosphine)gold(I) chloride / chloroform-d1; d(4)-methanol / 1.33 h / 30 °C
With
N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; (4-fluorophenyl)-λ3-iodanediyl diacetate; (1S)-10-camphorsulfonic acid; acetic acid;
In
chloroform-d1; chloroform; d(4)-methanol;
DOI:10.1021/ja408712e