Technology Process of C41H50N4O6S
There total 6 articles about C41H50N4O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C38H45N3O5;
With
1,1'-carbonyldiimidazole;
In
tetrahydrofuran;
at 50 ℃;
for 1h;
Inert atmosphere;
cyclopropanesulphonamide;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran;
at 125 ℃;
for 1h;
Sealed tube;
With
trifluoroacetic acid;
In
tetrahydrofuran;
DOI:10.1139/cjc-2012-0319
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / 85 °C / Inert atmosphere
2.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere
3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere
3.2: 50 °C / pH 4 - 5
4.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere
4.2: 1 h / 125 °C / Sealed tube
With
hydrogenchloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; trifuran-2-yl-phosphane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; dimethyl sulfoxide;
1.1: |Suzuki-Miyaura Coupling;
DOI:10.1139/cjc-2012-0319
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere
1.2: 50 °C / pH 4 - 5
2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere
2.2: 1 h / 125 °C / Sealed tube
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1139/cjc-2012-0319
