C₂₂H₂₈O₄S

Base Information

Chemical Name:C₂₂H₂₈O₄S
CAS No.:137105-64-7
Molecular Formula:C₂₂H₂₈O₄S
Molecular Weight:388.528
Hs Code.:

C<sub>22</sub>H<sub>28</sub>O<sub>4</sub>S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₈O₄S

Chemical Property:

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Technology Process of C₂₂H₂₈O₄S

There total 5 articles about C₂₂H₂₈O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 137105-64-7
C₂₂H₂₈O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 45 min; 2) DMF, overnight

2: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1) CH₂Cl₂, -60 deg C, 15 min; 2) Ch₂Cl₂, -60 deg C, 5 min

3: 1.) BuLi / 1) DME, hexane, -70 deg C, 20 min; 2) DME, hexane, -70 deg C, 10 min, -70 deg C --> room temperature, reflux (24 h)

With n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; triethylamine;

Reference yield:

: 58378-33-9
o-anisaldehyde dimethyl acetal

: 137105-64-7
C₂₂H₂₈O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / boron trifluoride-diethyl ether / CH₂Cl₂ / 1) -20 deg C --> room temperature; 2) room temperature, overnight

2: 1.) BuLi / 1) DME, hexane, -70 deg C, 20 min; 2) DME, hexane, -70 deg C, 10 min, -70 deg C --> room temperature, reflux (24 h)

With n-butyllithium; boron trifluoride diethyl etherate; In dichloromethane;

Reference yield:

: 147-93-3
Thiosalicylic acid

: 137105-64-7
C₂₂H₂₈O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

2: 1.) NaH / 1.) DMF, 45 min; 2) DMF, overnight

3: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1) CH₂Cl₂, -60 deg C, 15 min; 2) Ch₂Cl₂, -60 deg C, 5 min

4: 1.) BuLi / 1) DME, hexane, -70 deg C, 20 min; 2) DME, hexane, -70 deg C, 10 min, -70 deg C --> room temperature, reflux (24 h)

With lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; triethylamine; In diethyl ether;