methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane

Base Information

• Chemical Name: methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane
• CAS No.: 303128-88-3
• Molecular Formula: C₁₄H₂₆GeOSSi
• Molecular Weight: 343.101
• Mol file: 303128-88-3.mol

Synonyms:

Chemical Property of methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane

There total 1 articles about methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chloro-trimethyl-silane (75-77-4) + methoxy(phenylsulfanyl)(trimethylgermyl)methane (303128-86-1) → methoxy(phenylsulfanyl)(trimethylgermyl)(trimethylsilyl)methane (303128-88-3)

Guidance literature:

With tert.-butyl lithium; In tetrahydrofuran; N2; t-BuLi added dropwise to a soln. of 2 at -78°C, stirred at -78°C for 30 min, a soln. of Si comp. added dropwise, stirred for 2 h, at ambient temp.; aq. NH4Cl added, extd. (benzene), washed (H2O), dried (MgSO4), evapd., chromy. (silica gel, hexane-CHCl3 5:1);

DOI:10.1039/b003016n

upstream raw materials:

chloro-trimethyl-silane

methoxy(phenylsulfanyl)(trimethylgermyl)methane