2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

Base Information

Chemical Name:2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide
CAS No.:1269802-69-8
Molecular Formula:C₄₄H₅₃ClN₃*I
Molecular Weight:786.282
Hs Code.:

2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

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Chemical Property of 2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

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Technology Process of 2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

There total 6 articles about 2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1269802-53-0
1-formyl-2-chloro-3-hydroxymethylene-5-(4-diethylaminophenyl)cyclohexene

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

: 1269802-69-8
2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

Guidance literature:: In butan-1-ol; benzene; for 4h; Reflux;

Reference yield:

: 124500-60-3
4-(4-nitrophenyl)cyclohexan-1-one

: 1269802-69-8
2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 7 h / 50 °C

2: sodium carbonate / isopropyl alcohol / 6 h / Reflux

3: trichlorophosphate / dichloromethane / 5 h / 0 - 5 °C / Reflux

4: butan-1-ol; benzene / 4 h / Reflux

With palladium 10% on activated carbon; hydrogen; sodium carbonate; trichlorophosphate; In dichloromethane; isopropyl alcohol; butan-1-ol; benzene;

Reference yield:

: 124500-61-4
4-(4-aminophenyl)-cyclohexanone

: 1269802-69-8
2-[2-chloro-3-[2-(1,3-dihydro-1-ethyl-3,3-dimethyl-2H-indolidine)ethyl-1-cyclohexyl]ethyl-5-(4-diethylamino)benzene]-1-ethyl-3,3-dimethylindoline iodide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / isopropyl alcohol / 6 h / Reflux

2: trichlorophosphate / dichloromethane / 5 h / 0 - 5 °C / Reflux

3: butan-1-ol; benzene / 4 h / Reflux

With sodium carbonate; trichlorophosphate; In dichloromethane; isopropyl alcohol; butan-1-ol; benzene;