Technology Process of 5-methoxy-2-<(4-methoxybenzoyl)amino>acetophenone
There total 6 articles about 5-methoxy-2-<(4-methoxybenzoyl)amino>acetophenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
for 1h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) K2CO3 / 1.) THF, 1 h, 2.) THF, reflux, 24 h
2: 88 percent / tetrahydrofuran / 1.) -50 deg C, 4 h, 2.) r.t., 1 h
3: 88 percent / PDC / CH2Cl2 / 6 h / Heating
4: 97 percent / H2 / 5percent Pd/C / ethanol / 3 h / 760 Torr
5: 77 percent / pyridine / CH2Cl2 / 1 h / Ambient temperature
With
pyridine; dipyridinium dichromate; hydrogen; potassium carbonate;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 88 percent / tetrahydrofuran / 1.) -50 deg C, 4 h, 2.) r.t., 1 h
2: 88 percent / PDC / CH2Cl2 / 6 h / Heating
3: 97 percent / H2 / 5percent Pd/C / ethanol / 3 h / 760 Torr
4: 77 percent / pyridine / CH2Cl2 / 1 h / Ambient temperature
With
pyridine; dipyridinium dichromate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane;
