C₁₇H₂₃NO₄

Base Information

• Chemical Name: C₁₇H₂₃NO₄
• CAS No.: 158091-91-9
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Mol file: 158091-91-9.mol

Synonyms:

Chemical Property of C₁₇H₂₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₄

There total 16 articles about C₁₇H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2,2-dimethyl-1,3-dioxolane-4-carboxylate (108865-84-5) → C17H23NO4 (158091-91-9)

Guidance literature:

Multi-step reaction with 8 steps

1.1: lithium diisopropylamine / diethyl ether / 0.17 h / -78 °C

1.2: diethyl ether / 0.5 h

2.1: Et₃N / CH₂Cl₂ / 1.5 h

3.1: 75 percent / LiAlH₄ / diethyl ether / 20 h / 20 °C

4.1: NaH / tetrahydrofuran / 1 h

4.2: 81 percent / tetrahydrofuran / 20 h / Heating

5.1: 1.38 g / potassium carbonate / acetone / 5 h / Heating

6.1: 70 percent / LiAlH₄ / diethyl ether / 2 h

7.1: 245 mg / dimethyl sulfoxide; oxalyl chloride / CH₂Cl₂ / 1 h / -78 °C

8.1: diethyl ether / 1 h

With lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; 1.1: Metallation / 1.2: Condensation / 2.1: Elimination / 3.1: Reduction / 4.1: Metallation / 4.2: Alkylation / 5.1: Esterification / 6.1: Reduction / 7.1: Oxidation / 8.1: Condensation;

DOI:10.1039/a905802h

Reference yield:

(2,2-Dimethyl-4-vinyl-[1,3]dioxolan-4-ylmethoxy)-acetic acid (257949-99-8) → C17H23NO4 (158091-91-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.38 g / potassium carbonate / acetone / 5 h / Heating

2: 70 percent / LiAlH₄ / diethyl ether / 2 h

3: 245 mg / dimethyl sulfoxide; oxalyl chloride / CH₂Cl₂ / 1 h / -78 °C

4: diethyl ether / 1 h

With lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; In diethyl ether; dichloromethane; acetone; 1: Esterification / 2: Reduction / 3: Oxidation / 4: Condensation;

DOI:10.1039/a905802h

Reference yield:

(4-ethenyl-2,2-dimethyl-1,3-dioxolan-4-yl)methanol (257949-76-1) → C17H23NO4 (158091-91-9)

Guidance literature:

Multi-step reaction with 5 steps

1.1: NaH / tetrahydrofuran / 1 h

1.2: 81 percent / tetrahydrofuran / 20 h / Heating

2.1: 1.38 g / potassium carbonate / acetone / 5 h / Heating

3.1: 70 percent / LiAlH₄ / diethyl ether / 2 h

4.1: 245 mg / dimethyl sulfoxide; oxalyl chloride / CH₂Cl₂ / 1 h / -78 °C

5.1: diethyl ether / 1 h

With lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; 1.1: Metallation / 1.2: Alkylation / 2.1: Esterification / 3.1: Reduction / 4.1: Oxidation / 5.1: Condensation;

DOI:10.1039/a905802h

upstream raw materials:

N-benzyloxyamine

(2,2-Dimethyl-4-vinyl-[1,3]dioxolan-4-ylmethoxy)-acetaldehyde

methyl 2,2-dimethyl-1,3-dioxolane-4-carboxylate

(4-ethenyl-2,2-dimethyl-1,3-dioxolan-4-yl)methanol