o-boronobenzalmethoxyamine

Base Information

Chemical Name:o-boronobenzalmethoxyamine
CAS No.:160161-70-6
Molecular Formula:C₈H₁₀BNO₃
Molecular Weight:178.983
Hs Code.:

Synonyms:

Suppliers and Price of o-boronobenzalmethoxyamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-boronobenzalmethoxyamine

Chemical Property:

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Technology Process of o-boronobenzalmethoxyamine

There total 3 articles about o-boronobenzalmethoxyamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 40138-16-7
2-formylbenzene boronic acid

: 593-56-6
N-methoxylamine hydrochloride

: 160161-70-6
o-boronobenzalmethoxyamine

Guidance literature:: With NaOH; In water; o-formylbenzeneboronic acid and methoxyamine hydrochloride added to water, pH adjusted to 7 with 10% NaOH, refluxed for 15 min, cooled to room temp.; placed at 4°C overnight, recrystd. from water;
DOI:10.1007/BF01671677

Reference yield:

: 40138-16-7
2-formylbenzene boronic acid

: 593-56-6
N-methoxylamine hydrochloride

: 160161-70-6
o-boronobenzalmethoxyamine

: C₈H₁₀BNO₃

Guidance literature:: In aq. phosphate buffer; dimethyl sulfoxide; at 20 ℃; pH=7.4; Overall yield = 43 percent; Overall yield = 206 mg;
DOI:10.1039/d1ob01668g

Reference yield:

: o-tolueneboronic anhydride

: 160161-70-6
o-boronobenzalmethoxyamine

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / tetrachloromethane

2: NaOH / water

With bromine; NaOH; In tetrachloromethane; water;
DOI:10.1007/BF01671677