2,11-bisbenzophenantrene

Base Information

Chemical Name:2,11-bisbenzophenantrene
CAS No.:65796-61-4
Molecular Formula:C₄₈H₃₀F₁₂P₂
Molecular Weight:896.695
Hs Code.:

2,11-bis<bis(3-trifluoromethylphenyl)phosphinomethyl>benzo<c>phenantrene

Synonyms:

Suppliers and Price of 2,11-bisbenzophenantrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,11-bisbenzophenantrene

Chemical Property:

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Technology Process of 2,11-bisbenzophenantrene

There total 3 articles about 2,11-bisbenzophenantrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15929-44-9
bis(α,α,α-trifluoro-3-tolyl)phosphine oxide

: 65796-61-4
2,11-bisbenzophenantrene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / SiHCl₃ / acetonitrile; triethylamine / 3 h / 70 °C

2: 1.) Na / 1.) liq. NH₃, 1 h; 2.) diethyl ether

With trichlorosilane; sodium; In triethylamine; acetonitrile;
DOI:10.1002/hlca.19830660607

Reference yield:

: 401-78-5
3-bromo-1-trifluoromethylbenzene

: 65796-61-4
2,11-bisbenzophenantrene

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Mg, Et₂O, (ii) HPO(OEt)2, (iii) aq. HCl

2: LiAlH₄ / diethyl ether / Heating

3: (i) nBuLi, hexane, THF, (ii) /BRN= 2535167/

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1002/hlca.19770600835