dichlorotitanium phthalocyanine

Base Information

• Chemical Name: dichlorotitanium phthalocyanine
• CAS No.: 1208497-30-6
• Molecular Formula: C₃₂H₁₆Cl₂N₈Ti
• Molecular Weight: 631.319
• Mol file: 1208497-30-6.mol

Synonyms:

Chemical Property of dichlorotitanium phthalocyanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dichlorotitanium phthalocyanine

There total 5 articles about dichlorotitanium phthalocyanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

titanium tetrachloride (7550-45-0) + phthalonitrile (91-15-6) + 2-Methylnaphthalene (91-57-6,34468-07-0) → titanium(IV) chloride phthalocyaninate (1208497-30-6,16903-42-7)

Guidance literature:

In further solvent(s); byproducts: HCl, C10H6CH3Cl; ligands were dissolved in 2-bromonaphthalene under heating, TiCl4 was added, heated to 220°C for 1 h, cooled to 50°C; washed with benzene and MeOH, dried in air at room temp.; elem. anal.;

Reference yield: 60.0%

29H,31H-phthalocyanine (574-93-6) + titanium tetrachloride (7550-45-0) → titanium(IV) chloride phthalocyaninate (1208497-30-6,16903-42-7)

Guidance literature:

In further solvent(s); the soln. of ligand in hot α-chloronaphthalene and TiCl4 was heated at 220°C for 10 h with stirring under N2; the soln. was cooled, ppt. was filtered off, washed with methanol, elem. anal.;

Reference yield:

titanium tetrachloride (7550-45-0) + phthalonitrile (91-15-6) → titanium(IV) chloride phthalocyaninate (1208497-30-6,16903-42-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pentan-1-ol; for 7h; Heating / reflux;

upstream raw materials:

titanium tetrachloride

phthalonitrile

29H,31H-phthalocyanine

2-Methylnaphthalene

Downstream raw materials:

oxotitanium(IV) phthalocyanine

oxo(phthalocyaninato)titanium(IV)

titanium(IV) oxide phthalocyaninate

titanium(IV) oxide phthalocyaninate