tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

Base Information

Chemical Name:tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)
CAS No.:102513-04-2
Molecular Formula:C₁₉H₁₉IMnO₄PSi
Molecular Weight:552.259
Hs Code.:

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Chemical Property of tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

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Technology Process of tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

There total 1 articles about tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 14879-42-6
iodo(pentacarbonyl)manganese(I)

: 17154-34-6
(trimethylsilyl)diphenylphosphine

: 102513-04-2
tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

Guidance literature:: In toluene; byproducts: CO; dropwise addn. of silylphosphane to Mn complex soln. at room temp.; stirring, 25°C, 12h; distg. off trimethylsilyl halogenide and solvent; dissoln. of residue in petroleum ether/toluene (2/1); evapn.; cooling to -30°C; crystn.; elem. anal.;

Reference yield: 62.0%

: 102513-04-2
tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

: 407-25-0
trifluoroacetic anhydride

: 128239-84-9
tetracarbonyliodo(trifluoroacetyldiphenylphosphane)manganese(I)

Guidance literature:: In toluene; byproducts: (CH3)3SiO2CCF3; addn. of (CF3CO)2O to Mn complex soln. under Ar excluding air and moisture; stirring, 25°C, several h; evapn.; recrystn. (toluene:petroleum ether 60:90, -30°C); elem. anal.;

Reference yield: 45.0%

: 102513-04-2
tetracarbonyliodo(trimethylsilyldiphenylphosphane)manganese(I)

: 21280-43-3
1-adamantanesulphinyl chloride

: 128268-20-2
tetracarbonyliodo(adamantanesulfinyldiphenylphosphane)manganese(I)

Guidance literature:: In toluene; byproducts: (CH3)3SiCl; slow dropwise addn. of sulfinyl chloride soln. to Mn complex soln. with stirring under Ar excluding air and moisture, 25°C, 30 min; column chromy.; evapn.; elem. anal.;