(2-ClHgC₆H₄)Ph₂P=N(t)Bu

Base Information

Chemical Name:(2-ClHgC₆H₄)Ph₂P=N(t)Bu
CAS No.:1180491-92-2
Molecular Formula:C₂₂H₂₃ClHgNP
Molecular Weight:568.448
Hs Code.:

(2-ClHgC<sub>6</sub>H<sub>4</sub>)Ph<sub>2</sub>P=N(t)Bu

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Chemical Property of (2-ClHgC₆H₄)Ph₂P=N(t)Bu

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Technology Process of (2-ClHgC₆H₄)Ph₂P=N(t)Bu

There total 1 articles about (2-ClHgC₆H₄)Ph₂P=N(t)Bu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 13989-64-5
triphenylphosphine-N-tertbutylimine

: 1600-27-7
mercury(II) diacetate

: lithium chloride

: 1180491-92-2
(2-ClHgC₆H₄)Ph₂P=N(t)Bu

Guidance literature:: In tetrahydrofuran; (N2); Ph3P=N(t)Bu and Hg(OAc)2 were refluxed in THF for 16 h, allowed tocool, LiCl was added, stirred for 4 h; filtered, evapd., crystd. from CH2Cl2/Et2O at -20°C;
DOI:10.1016/j.ica.2009.04.024

Reference yield: 74.0%

: 53514-38-8
tetramethylammonium tetrachloroaurate(III)

: 1180491-92-2
(2-ClHgC₆H₄)Ph₂P=N(t)Bu

: 75-57-0
tetramethlyammonium chloride

: 1180491-95-5
(2-Cl₂AuC₆H₄)Ph₂P=N(t)Bu

Guidance literature:: In acetonitrile; (dark); mercury complex, Me4N(AuCl4) and Me4NCl were added to MeCN, stirred for 48 h; evapd., extd. with CH2Cl2, filtered, Et2O was added to fitrate, crystd. at -20°C, elem. anal.;
DOI:10.1016/j.ica.2009.04.024

Reference yield:

: 1180491-92-2
(2-ClHgC₆H₄)Ph₂P=N(t)Bu

: 1180491-99-9
((C₆H₄S(COO))AuC₆H₄)(C₆H₅)2PNC(CH₃)3

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: (CH₃)3N / methanol

With (CH₃)3N; In methanol; acetonitrile;
DOI:10.1016/j.ica.2009.04.024