Technology Process of Hexabutylbenzene
There total 3 articles about Hexabutylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; chloro-trimethyl-silane;
In
tetrahydrofuran;
for 6h;
Heating;
DOI:10.1021/jo00382a039
- Guidance literature:
-
5-decyne;
With
titanocene dichloride; diethylaluminium chloride; magnesium;
In
tetrahydrofuran;
at 21 - 22 ℃;
for 8h;
With
diclazuril;
In
tetrahydrofuran; water-d2;
DOI:10.1023/A:1025697110484
- Guidance literature:
-
With
1,3-bis-(diphenylphosphino)propane; cobalt(II) chloride; zinc powder;
In
2-methyltetrahydrofuran;
at 80 ℃;
for 24h;
Reagent/catalyst;
Temperature;
Solvent;
Overall yield = 83 percent; stereoselective reaction;
DOI:10.1021/acscatal.2c00181
