N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine

Base Information

• Chemical Name: N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine
• CAS No.: 16574-36-0
• Molecular Formula: C15H19 N
• Molecular Weight: 213.323
• Mol file: 16574-36-0.mol

Synonyms:2-Naphthalenemethylamine,N,N-diethyl- (8CI); N,N-Diethyl-2-naphthylmethylamine

Chemical Property of N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine

Chemical Property:

• Vapor Pressure: 0.000584mmHg at 25°C
• Boiling Point: 310.9°C at 760 mmHg
• Flash Point: 129.2°C
• Density: 1g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine

There total 6 articles about N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

diethylamine (109-89-7) + 2-bromomethylnaphthyl bromide (939-26-4) → N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine (16574-36-0)

Guidance literature:

diethylamine; 2-bromomethylnaphthyl bromide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With sodium hydroxide; In water;

DOI:10.1016/j.tet.2010.03.040

Reference yield: 87.0%

β-naphthaldehyde (66-99-9) + diethylamine (109-89-7) → N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine (16574-36-0)

Guidance literature:

With piperidin-2-one; sodium tetrahydroborate; N,N-diisopropyl-4H-benzo[d][1,3,2]dioxaborinin-2-amine; In 1,2-dichloro-ethane; at 20 ℃;

DOI:10.1055/s-2006-939070

Reference yield: 9.0%

N,N-diethyl-2-naphthamide (13577-84-9) → N-ethyl-N-(naphthalen-2-ylmethyl)ethanamine (16574-36-0) + N,N,N',N'-Tetraethyl-1,2-di(2'-naphthyl)ethylendiamin + 1,2-bis(diethylamino)-1,2-bis(2-naphthyl)ethane

Guidance literature:

With titanocene difluoride; methylphenylsilane; In toluene; at 80 ℃;

DOI:10.1002/1521-3773(20010601)40:11<2129::AID-ANIE2129>3.0.CO;2-2

upstream raw materials:

N,N-diethyl-2-naphthamide

β-naphthaldehyde

diethylamine

2-bromomethylnaphthyl bromide

Downstream raw materials:

2-Diaethylamino-maleinsaeure-dimethylester, 2-Diaethylamino-fumarsaeure-dimethylester

benzoic acid 2-naphthalenylmethyl ester