trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

Base Information

Chemical Name:trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether
CAS No.:110355-41-4
Molecular Formula:C₁₄H₂₀O₃S
Molecular Weight:268.377
Hs Code.:

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Chemical Property of trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

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Technology Process of trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

There total 4 articles about trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34452-56-7
trimethylsilyl p-tolylsulfonylacetylene

: 110355-41-4
trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / diethyl ether / 1.) -78 deg C, 30 min, 2.) 25 deg C, 12 h

2: 99 percent / benzene / 2 h / Irradiation

3: 1.) Na / 1.) 25 deg C, 2.) 25 deg C, 30 min

With sodium; In diethyl ether; benzene;
DOI:10.1021/jo00230a020

Reference yield:

: 110355-39-0
3,3-dimethyl-4-(p-tolylsulfonyl)-5-(trimethylsilyl)-3H-pyrazole

: 110355-41-4
trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / benzene / 2 h / Irradiation

2: 1.) Na / 1.) 25 deg C, 2.) 25 deg C, 30 min

With sodium; In benzene;
DOI:10.1021/jo00230a020

Reference yield:

: 110355-40-3
[1-Diazo-3-methyl-2-(toluene-4-sulfonyl)-but-2-enyl]-trimethyl-silane

: 110355-41-4
trans-2,2-dimethyl-3-(p-tolylsulfonyl)cyclopropyl ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / Irradiation

2: 1.) Na / 1.) 25 deg C, 2.) 25 deg C, 30 min

With sodium; In benzene;
DOI:10.1021/jo00230a020