Technology Process of C45H67FN4O9
There total 4 articles about C45H67FN4O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(acetonitrile)copper(I) hexafluorophosphate; bathophenantrolinedisulfonic acid disodium salt;
at 60 ℃;
for 0.0833333h;
Solvent;
Reagent/catalyst;
Concentration;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA / water; acetonitrile
2: bathophenantrolinedisulfonic acid disodium salt; tetrakis(acetonitrile)copper(I) hexafluorophosphate / 0.08 h / 60 °C
With
tetrakis(acetonitrile)copper(I) hexafluorophosphate; bathophenantrolinedisulfonic acid disodium salt; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA;
In
water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide / acetonitrile / 5 h / 120 °C
2: caesium carbonate / dichloromethane / 24 h / 20 °C
3: [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA / water; acetonitrile
4: bathophenantrolinedisulfonic acid disodium salt; tetrakis(acetonitrile)copper(I) hexafluorophosphate / 0.08 h / 60 °C
With
sodium azide; tetrakis(acetonitrile)copper(I) hexafluorophosphate; bathophenantrolinedisulfonic acid disodium salt; caesium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA;
In
dichloromethane; water; acetonitrile;