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Technology Process of C5H5CoC6H4Si2(C6H5)2(CH3)4

C5H5CoC6H4Si2(C6H5)2(CH3)4

Base Information
  • Chemical Name:C5H5CoC6H4Si2(C6H5)2(CH3)4
  • CAS No.:301317-63-5
  • Molecular Formula:C27H31CoSi2
  • Molecular Weight:470.707
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>CoC<sub>6</sub>H<sub>4</sub>Si<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2(CH<sub>3</sub>)4

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Chemical Property of C5H5CoC6H4Si2(C6H5)2(CH3)4
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Technology Process of C5H5CoC6H4Si2(C6H5)2(CH3)4

There total 1 articles about C5H5CoC6H4Si2(C6H5)2(CH3)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

dicarbonylcyclopentadienylcobalt
12078-25-0,12078-23-8

dicarbonylcyclopentadienylcobalt

1,8-diphenyl-3,6-disila-1,7-octadiyne

1,8-diphenyl-3,6-disila-1,7-octadiyne

C<sub>5</sub>H<sub>5</sub>CoC<sub>6</sub>H<sub>4</sub>Si<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2(CH<sub>3</sub>)4
301317-63-5

C5H5CoC6H4Si2(C6H5)2(CH3)4

Guidance literature:
In octane; in refluxing octane; elem. anal.;
DOI:10.1246/cl.2000.896

Reference yield: 99.0%

1,2-dimethoxyethane
110-71-4

1,2-dimethoxyethane

C<sub>5</sub>H<sub>5</sub>CoC<sub>6</sub>H<sub>4</sub>Si<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2(CH<sub>3</sub>)4
301317-63-5

C5H5CoC6H4Si2(C6H5)2(CH3)4

lithium
7439-93-2

lithium

Li(1,2-dimethoxyethane)2[C<sub>6</sub>H<sub>4</sub>Si<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2(CH<sub>3</sub>)4]

Li(1,2-dimethoxyethane)2[C6H4Si2(C6H5)2(CH3)4]

Guidance literature:
In tetrahydrofuran; mixture stirred at room temp. to give a dark brown soln. within 24 h; solvent removed in vacuo, degassed hexane added, Li and insoluble dark materials removed, solution cooled to afford the product (THF ligand), ligand exchange on the Li(1+) ions from THF to 1,2-dimethoxyethane (DME), crystn. from heptane at -30°C;
DOI:10.1246/cl.2000.896
upstream raw materials:

dicarbonylcyclopentadienylcobalt

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