C₂₆H₂₅NO₅S

Base Information

Chemical Name:C₂₆H₂₅NO₅S
CAS No.:1616088-56-2
Molecular Formula:C₂₆H₂₅NO₅S
Molecular Weight:463.554
Hs Code.:

C<sub>26</sub>H<sub>25</sub>NO<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₅NO₅S

Chemical Property:

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Technology Process of C₂₆H₂₅NO₅S

There total 3 articles about C₂₆H₂₅NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616087-99-0
C₂₁H₁₉NO₃S

: 140-88-5,9003-32-1
ethyl acrylate

: 1616088-56-2
C₂₆H₂₅NO₅S

: 1616088-57-3
N-[2-(3-ethoxy-3-oxopropyl)-5-(phenoxymethyl)benzoyl]-Smethyl-S-phenylsulfoximine

Guidance literature:: With silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate hydrate; In 1,2-dichloro-ethane; at 120 ℃; for 24h; Overall yield = 66 %; Overall yield = 2.1 g; regioselective reaction; Inert atmosphere; Glovebox; Schlenk technique;
DOI:10.1021/jo5008465

Reference yield:

: 1193-82-4
racemic methyl phenyl sulfoxide

: 1616088-56-2
C₂₆H₂₅NO₅S

: 1616088-57-3
N-[2-(3-ethoxy-3-oxopropyl)-5-(phenoxymethyl)benzoyl]-Smethyl-S-phenylsulfoximine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; sulfuric acid / chloroform / Schlenk technique

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

3: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate hydrate; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 120 °C / Inert atmosphere; Glovebox; Schlenk technique

With dmap; silver hexafluoroantimonate; sodium azide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate hydrate; sulfuric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; chloroform; 1,2-dichloro-ethane;
DOI:10.1021/jo5008465

Reference yield:

: 4381-25-3
S-methyl-S-phenylsulfoximine

: 1616088-56-2
C₂₆H₂₅NO₅S

: 1616088-57-3
N-[2-(3-ethoxy-3-oxopropyl)-5-(phenoxymethyl)benzoyl]-Smethyl-S-phenylsulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate hydrate; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 120 °C / Inert atmosphere; Glovebox; Schlenk technique

With dmap; silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo5008465