[1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-

Base Information

Chemical Name:[1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-
CAS No.:107777-49-1
Molecular Formula:C14H14O4
Molecular Weight:246.263
Hs Code.:
DSSTox Substance ID:DTXSID40438787
Nikkaji Number:J817.784H
Wikidata:Q82254611
Mol file:107777-49-1.mol

Synonyms:[1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-;107777-49-1;2,2'-Bi[3-methoxyphenol];DTXSID40438787

Suppliers and Price of [1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:246.08920892
Heavy Atom Count:18
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1C2=C(C=CC=C2OC)O)O

Technology Process of [1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy-

There total 3 articles about [1,1'-Biphenyl]-2,2'-diol, 6,6'-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57234-28-3
1-methoxy-3-(methoxymethoxy)benzene

: 107777-49-1
2,2’-dihydroxy-6,6’-dimethoxy-1,1’-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 20 °C / Inert atmosphere

1.2: 12 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / methanol / 1 h / 70 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/acs.joc.6b01645