(Zn(SC₆H₅)4)^(2-)*2((C₆H₁₁)2NH₂)⁽¹⁺⁾

Base Information

• Chemical Name: (Zn(SC₆H₅)4)^(2-)*2((C₆H₁₁)2NH₂)⁽¹⁺⁾
• CAS No.: 130574-96-8
• Molecular Formula: 2C₁₂H₂₃N*C₂₄H₂₀S₄Zn*2H
• Molecular Weight: 866.735
• Mol file: 130574-96-8.mol

Synonyms:

Chemical Property of (Zn(SC₆H₅)4)^(2-)*2((C₆H₁₁)2NH₂)⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Zn(SC₆H₅)4)^(2-)*2((C₆H₁₁)2NH₂)⁽¹⁺⁾

There total 1 articles about (Zn(SC₆H₅)4)^(2-)*2((C₆H₁₁)2NH₂)⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

sodium thiophenolate (930-69-8) + dicyclohexylamine hydrochloride (4693-92-9) + zinc(II) chloride (7646-85-7,24359-56-6) → (Zn(SC6H5)4)(2-)*2((C6H11)2NH2)(1+) (130574-96-8)

Guidance literature:

In methanol; byproducts: NaCl; C6H5SNa and anhyd. ZnCl2 was dissolved in MeOH, white ppt. was formed, solvent was removed under vac. and replaced of CH3CN; (Cy2NH2)Cl was added, mixt. was stirring overnigth in an inert atm.;; NaCl was filtered, filtrate was cooled to 0°C to initiate crystn., after 1.5 h product was isolated by decanting the soln., washed with ether, dried in vac.; elem. anal.;;

DOI:10.1021/ja00002a021

upstream raw materials:

sodium thiophenolate

dicyclohexylamine hydrochloride

zinc(II) chloride