2-tosyl-2,6-diazaspiro[3.3]heptane

Base Information

Chemical Name:2-tosyl-2,6-diazaspiro[3.3]heptane
CAS No.:1333960-25-0
Molecular Formula:C₁₂H₁₆N₂O₂S
Molecular Weight:252.337
Hs Code.:2933998090
Mol file:1333960-25-0.mol

Synonyms:

Suppliers and Price of 2-tosyl-2,6-diazaspiro[3.3]heptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Tosyl-2,6-diazaspiro[3.3]heptane 95+%
1g
$ 794.00

Chemenu
2-Tosyl-2,6-diazaspiro[3.3]heptane 95%
1g
$ 750.00

American Custom Chemicals Corporation
2-TOSYL-2,6-DIAZASPIRO[3.3]HEPTANE 95.00%
5MG
$ 451.98

Alichem
2-Tosyl-2,6-diazaspiro[3.3]heptane
1g
$ 870.35

Total 3 raw suppliers

Chemical Property of 2-tosyl-2,6-diazaspiro[3.3]heptane

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-Tosyl-2,6-diazaspiro[3.3]heptane 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-tosyl-2,6-diazaspiro[3.3]heptane

There total 6 articles about 2-tosyl-2,6-diazaspiro[3.3]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1041026-64-5
2-benzyl-6-(p-toluenesulfonyl)-2,6-diazaspiro[3.3]heptane

: 1333960-25-0
C₁₂H₁₆N₂O₂S

Guidance literature:: With 10% Pd on charcoal; hydrogen; In methanol; at 45 ℃; for 53h;
DOI:10.1021/ol801293f

Reference yield:

: 1522-92-5
2,2-bis(bromomethyl)-3-bromo-propan-1-ol

: 1333960-25-0
C₁₂H₁₆N₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / ethanol / 48 h / 25 - 100 °C

2: hydrogen bromide; acetic acid / diethyl ether / 0.5 h / 20 °C

3: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / Reflux

5: hydrogen; palladium 10% on activated carbon / methanol / 48 h / 45 °C / 2585.81 Torr

With carbon tetrabromide; palladium 10% on activated carbon; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; potassium hydroxide; In methanol; diethyl ether; ethanol; dichloromethane; acetonitrile;

Reference yield:

: 13573-28-9
6-(p-toluenesulfonyl)-2-oxa-6-azaspiro[3.3]heptane

: 1333960-25-0
C₁₂H₁₆N₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen bromide; acetic acid / diethyl ether / 0.5 h / 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / Reflux

4: hydrogen; palladium 10% on activated carbon / methanol / 48 h / 45 °C / 2585.81 Torr

With carbon tetrabromide; palladium 10% on activated carbon; hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In methanol; diethyl ether; dichloromethane; acetonitrile;