Technology Process of 2-anilino-6-chloropurine sodium salt
There total 4 articles about 2-anilino-6-chloropurine sodium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
acetonitrile;
for 0.333333h;
Ambient temperature;
DOI:10.1021/jm00403a004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / 2-methoxy-ethanol / Heating
2: 74 percent / thionyl chloride / dimethylformamide / 1 h / 50 °C
3: sodium hydride / acetonitrile / 0.33 h / Ambient temperature
With
thionyl chloride; sodium hydride;
In
2-methoxy-ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00403a004
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 74 percent / thionyl chloride / dimethylformamide / 1 h / 50 °C
2: sodium hydride / acetonitrile / 0.33 h / Ambient temperature
With
thionyl chloride; sodium hydride;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00403a004
