[PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4

Base Information

• Chemical Name: [PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4
• CAS No.: 849334-27-6
• Molecular Formula: BF₄*C₂₈H₃₇O₃P₂PtS
• Molecular Weight: 797.498
• Mol file: 849334-27-6.mol

Synonyms:

Chemical Property of [PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4

There total 1 articles about [PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

thiophene (110-01-0) + silver tetrafluoroborate (14104-20-2) + chloromethyl(1,5-cyclooctadiene)platinum(II) + rac-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester (661459-86-5) → [PtMe(tetrahydrothiophene)(κ2-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester)]BF4 (849334-27-6)

Guidance literature:

In dichloromethane; under N2 atm. to soln. Pt complex and ligand in CH2Cl2 tetrahydrothiophene and AgBF4 were added and stirred at room temp. for 2 h; Celite was added and stirred for 15 min., soln. was filtered, evapd. in vac.; elem. anal.;

DOI:10.1021/ic0485559

upstream raw materials:

thiophene

silver tetrafluoroborate

rac-[(diphenylphosphinophenyl)methyl]phosphonic acid diethyl ester