L-Phenylalanine, N-acetyl-, 2-chloroethyl ester

Base Information

• Chemical Name: L-Phenylalanine, N-acetyl-, 2-chloroethyl ester
• CAS No.: 108395-58-0
• Molecular Formula: C13H16ClNO3
• Molecular Weight: 269.728

Synonyms:

Chemical Property of L-Phenylalanine, N-acetyl-, 2-chloroethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of L-Phenylalanine, N-acetyl-, 2-chloroethyl ester

There total 1 articles about L-Phenylalanine, N-acetyl-, 2-chloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-acetylamino-3-phenylpropanoic acid (2018-61-3) + 2-chloro-ethanol (107-07-3) → acetyl L-phenylalanine chloroethyl ester (108395-58-0)

Guidance literature:

With Amberlite IR-120;

Reference yield: 100.0%

ethanol (64-17-5) + acetyl L-phenylalanine chloroethyl ester (108395-58-0) → ethyl N-acetyl-(L)-phenylalaninate (2361-96-8)

Guidance literature:

With subtilisin Carlsberg; In carbon dioxide; at 38 ℃; for 2.5h; under 59280 - 60800 Torr;

DOI:10.1002/jccs.199900091

Reference yield: 86.0%

L-valinamide (4540-60-7,20108-78-5) + acetyl L-phenylalanine chloroethyl ester (108395-58-0) → N-Ac-L-Phe-L-Val-NH2

Guidance literature:

With porcine pancreatic lipase; In toluene; at 45 ℃; several days;

DOI:10.1021/ja00246a060

upstream raw materials:

(S)-2-acetylamino-3-phenylpropanoic acid

2-chloro-ethanol

Downstream raw materials:

N-acetyl-(S)-phenylalanine propyl ester

N-Ac-L-Phe-L-Leu-NH₂

(S)-2-Acetylamino-N-(6-hydroxy-hexyl)-3-phenyl-propionamide

1-O-(N-acetyl-L-phenylalanyl)castanospermine

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