C₄₅H₄₂ClNO₉

Base Information

Chemical Name:C₄₅H₄₂ClNO₉
CAS No.:1616766-82-5
Molecular Formula:C₄₅H₄₂ClNO₉
Molecular Weight:776.283
Hs Code.:

C<sub>45</sub>H<sub>42</sub>ClNO<sub>9</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₄₂ClNO₉

Chemical Property:

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Technology Process of C₄₅H₄₂ClNO₉

There total 11 articles about C₄₅H₄₂ClNO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1616766-80-3
C₃₀H₂₈Cl₂O₆

: 82157-46-8
C₁₅H₁₅NO₃

: 1616766-82-5
C₄₅H₄₂ClNO₉

Guidance literature:: With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; In tert-butyl alcohol; at 110 ℃; for 72h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c4cc01830c

Reference yield:

: 1616766-74-5
4-[(1Z,3E)-1-chloro-5-methylhexa-1,3,5-trien-1-yl]benzoic acid

: 1616766-82-5
C₄₅H₄₂ClNO₉

Guidance literature:: Multi-step reaction with 2 steps

1: (2-bromophenyl)boronic acid / 1,2-dichloro-ethane / 18 h / Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl / tert-butyl alcohol / 72 h / 110 °C / Molecular sieve; Inert atmosphere

With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; (2-bromophenyl)boronic acid; In 1,2-dichloro-ethane; tert-butyl alcohol; 1: |Diels-Alder Cycloaddition / 2: |Buchwald-Hartwig Coupling;
DOI:10.1039/c4cc01830c

Reference yield:

: 619-44-3
methyl 4-iodobenzoate

: 1616766-82-5
C₄₅H₄₂ClNO₉

Guidance literature:: Multi-step reaction with 7 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 18 h / 20 °C / Inert atmosphere

2: N-Bromosuccinimide; silver fluoride / acetonitrile / 18 h / 20 °C / Darkness

3: lithium chloride; bis(η3-allyl-μ-chloropalladium(II)); 1,5-cis,cis-cyclooctadiene; acetic acid / 18 h / 80 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 6 h / 20 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / tetrahydrofuran; water / 6 h / 50 °C / Darkness

6: (2-bromophenyl)boronic acid / 1,2-dichloro-ethane / 18 h / Reflux

7: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl / tert-butyl alcohol / 72 h / 110 °C / Molecular sieve; Inert atmosphere

With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; bis(η3-allyl-μ-chloropalladium(II)); lithium hydroxide monohydrate; silver fluoride; caesium carbonate; acetic acid; triethylamine; lithium chloride; (2-bromophenyl)boronic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; acetonitrile; tert-butyl alcohol; 1: |Sonogashira Cross-Coupling / 6: |Diels-Alder Cycloaddition / 7: |Buchwald-Hartwig Coupling;
DOI:10.1039/c4cc01830c