2,2-diphenyl-1,3,6,2-trithiaplumbocane

Base Information

• Chemical Name: 2,2-diphenyl-1,3,6,2-trithiaplumbocane
• CAS No.: 99225-66-8
• Molecular Formula: C₁₆H₁₈PbS₃
• Molecular Weight: 513.717
• Mol file: 99225-66-8.mol

Synonyms:

Chemical Property of 2,2-diphenyl-1,3,6,2-trithiaplumbocane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-diphenyl-1,3,6,2-trithiaplumbocane

There total 2 articles about 2,2-diphenyl-1,3,6,2-trithiaplumbocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

3-thiapentan-1,5-dithiol (3570-55-6) + diphenyllead(IV) diacetate (6928-68-3) → 2,2-diphenyl-1,3,6,2-trithiaplumbocane (99225-66-8)

Guidance literature:

With Na; In methanol; mixing and heating of Na and the ether; mixture is cooled to 0°C, addn. of the acetate with stirring;; pptn., after 15 min solvent is removed in vacuum and residue is redissolved in ether, filtn., crystn., elem. anal.;;

Reference yield:

3-thiapentan-1,5-dithiol (3570-55-6) + diphenyldiiodoplumbane (23351-01-1) → 2,2-diphenyl-1,3,6,2-trithiaplumbocane (99225-66-8)

Guidance literature:

In benzene; react. in the pesence of pyridine or triethylamine;;

upstream raw materials:

3-thiapentan-1,5-dithiol

diphenyldiiodoplumbane

diphenyllead(IV) diacetate