DIPHENYL LEAD DIACETATE

Base Information

• Chemical Name: DIPHENYL LEAD DIACETATE
• CAS No.: 6928-68-3
• Molecular Formula: C16H16 O4 Pb
• Molecular Weight: 479.501
• Hs Code.: 2931900090
• European Community (EC) Number: 230-052-1
• DSSTox Substance ID: DTXSID501047719
• NSC Number: 179769,173046
• Mol file: 6928-68-3.mol

Synonyms:Diphenylleaddiacetate (6CI); Lead, diacetoxydiphenyl- (7CI); Plumbane,bis(acetyloxy)diphenyl- (9CI); Plumbane, diacetoxydiphenyl- (8CI);Diacetatodiphenyllead; Diacetoxydiphenyllead; Diacetoxydiphenylplumbane;Diphenyldiacetoxylead; NSC 173046; NSC 179769

Chemical Property of DIPHENYL LEAD DIACETATE

Chemical Property:

• PSA: 52.60000
• LogP: 2.62040
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 480.08151
• Heavy Atom Count: 21
• Complexity: 335

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)O[Pb](C1=CC=CC=C1)(C2=CC=CC=C2)OC(=O)C

Technology Process of DIPHENYL LEAD DIACETATE

There total 11 articles about DIPHENYL LEAD DIACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

lead(IV) tetraacetate (546-67-8) + phenylboronic acid (98-80-6) → phenyllead(IV) triacetate (3076-54-8) + diphenyllead(IV) diacetate (6928-68-3)

Guidance literature:

In chloroform-d1; 40°C; not isolated; (1)H-NMR spectroscopy;

Reference yield:

silver(I) acetate (563-63-3) + diphenyllead(IV) dichloride (2117-69-3) → diphenyllead(IV) diacetate (6928-68-3)

Guidance literature:

In methanol; byproducts: AgCl; Pb compd. reacted with Ag salt in MeOH;

DOI:10.1002/zaac.200570052

Reference yield:

hexaphenyl diplumbane (3124-01-4) → lead acetate (301-04-2) + diphenyllead(IV) diacetate (6928-68-3)

Guidance literature:

With CH₃COOH; In not given; byproducts: C6H6; warming to 50-80°C (stirring), stirring (50-80°C, 3-20 h); cooling, addn. to ether/acetone (1:1), filtration off of Pb(OAc)2, solvent removal (20 Torr, 80°C);

DOI:10.1016/0022-328X(85)80302-8

upstream raw materials:

mercury(II) diacetate

Tetraphenyllead

diphenylmercury(II)

di-n-butyldiphenyltin

Downstream raw materials:

1-oxo-2-phenyl-2,3,4,5,6,7,8-heptafluoro-1,2-dihydronaphthalene

4-methyldiphenylamine

diphenyl lead sulfide

2,2-diphenyl-1,3,6,2-trithiaplumbocane