di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

Base Information

Chemical Name:di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate
CAS No.:1448338-45-1
Molecular Formula:C₃₁H₂₆O₄
Molecular Weight:462.545
Hs Code.:

Synonyms:

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Chemical Property of di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

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Technology Process of di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

There total 6 articles about di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62784-66-1
bis(1-naphthyl)methanol

: C₁₆H₁₅NO₆

: 1448338-45-1
di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

: (R)-di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

Guidance literature:: With BF₄^(1-)*C₂₁H₂₂N₃O⁽¹⁺⁾; caesium carbonate; In tetrahydrofuran; at 23 - 26 ℃; for 24h; Overall yield = 81 percent; Overall yield = 37.3 mg; enantioselective reaction; Schlenk technique; Molecular sieve; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00748

Reference yield:

: 7309-51-5
α-(2-methoxyphenoxy)propionic acid

: 62784-66-1
bis(1-naphthyl)methanol

: 46295-78-7
(R)-2-(2-methoxyphenoxy)propanoic acid

: 46295-80-1
(S)-2-(2-methoxyphenoxy)propanoic acid

: 1448338-45-1
di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

: (R)-di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

Guidance literature:: With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; 2,2-dimethylpropanoic anhydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.3987/COM-12-S(N)79

Reference yield:

: 66-77-3
1-naphthaldehyde

: 1448338-45-1
di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

: (R)-di(naphthalen-1-yl)methyl-2-(2-methoxyphenoxy)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium; iodine / tetrahydrofuran / 20 °C / Schlenk technique; Inert atmosphere

2: BF₄^(1-)*C₂₁H₂₂N₃O⁽¹⁺⁾; caesium carbonate / tetrahydrofuran / 24 h / 23 - 26 °C / Schlenk technique; Molecular sieve; Sealed tube; Inert atmosphere

With BF₄^(1-)*C₂₁H₂₂N₃O⁽¹⁺⁾; iodine; caesium carbonate; magnesium; In tetrahydrofuran;
DOI:10.1021/acs.orglett.0c00748