Technology Process of C37H53NO4Si2
There total 8 articles about C37H53NO4Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) Bu2BOTf, Et3N / 1.) toluene, -78 deg C, 2.) toluene, -78 deg C to 20 deg C
2: AlMe3 / CH2Cl2 / 20 °C
3: imidazole / dimethylformamide / 20 °C
4: DIBAL-H / toluene / -78 °C
5: NH2OH*HCl, NaOAc / ethanol; H2O / 20 °C
6: NaCNBH3 / methanol / 20 °C / pH 4
7: CH2Cl2 / 20 °C
With
1H-imidazole; di-n-butylboryl trifluoromethanesulfonate; hydroxylamine hydrochloride; trimethylaluminum; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; triethylamine;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: AlMe3 / CH2Cl2 / 20 °C
2: imidazole / dimethylformamide / 20 °C
3: DIBAL-H / toluene / -78 °C
4: NH2OH*HCl, NaOAc / ethanol; H2O / 20 °C
5: NaCNBH3 / methanol / 20 °C / pH 4
6: CH2Cl2 / 20 °C
With
1H-imidazole; hydroxylamine hydrochloride; trimethylaluminum; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: imidazole / dimethylformamide / 20 °C
2: DIBAL-H / toluene / -78 °C
3: NH2OH*HCl, NaOAc / ethanol; H2O / 20 °C
4: NaCNBH3 / methanol / 20 °C / pH 4
5: CH2Cl2 / 20 °C
With
1H-imidazole; hydroxylamine hydrochloride; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;