Cu⁽¹⁺⁾*(NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2*[B(C₆F₅)4]^(1-)=[Cu((NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2)][B(C₆F₅)4]

Base Information

• Chemical Name: Cu⁽¹⁺⁾*(NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2*[B(C₆F₅)4]^(1-)=[Cu((NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2)][B(C₆F₅)4]
• CAS No.: 1023595-89-2
• Molecular Formula: C₂₄BF₂₀*C₃₂H₃₁N₅*Cu
• Molecular Weight: 1228.22

Synonyms:

Chemical Property of Cu⁽¹⁺⁾*(NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2*[B(C₆F₅)4]^(1-)=[Cu((NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2)][B(C₆F₅)4]

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Technology Process of Cu⁽¹⁺⁾*(NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2*[B(C₆F₅)4]^(1-)=[Cu((NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2)][B(C₆F₅)4]

There total 1 articles about Cu⁽¹⁺⁾*(NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2*[B(C₆F₅)4]^(1-)=[Cu((NC₅H₄CH₂)2NCH₂C₅H₃NN(CH₂C₆H₅)2)][B(C₆F₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

tetrakis(acetonitrile)copper(I) tetrakis(pentafluorophenyl)borate (425370-02-1) + N(CH2C5H4N)2CH2C5H3NN(CH2C6H5)2 (1023595-98-3) → Cu(1+)*(NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2*[B(C6F5)4](1-)=[Cu((NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2)][B(C6F5)4] (1023595-89-2)

Guidance literature:

In tetrahydrofuran; under Ar; THF added with stirring to mixt. of ligand and Cu complex; pptd. by adding pentane; supernatant decanted; solid recrystd. from THF-pentane; washed with pentane; dried under vac.; elem. anal.;

DOI:10.1021/ic702437c

Reference yield: 74.0%

chloroform (67-66-3,8013-54-5) + Cu(1+)*(NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2*[B(C6F5)4](1-)=[Cu((NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2)][B(C6F5)4] (1023595-89-2) + water (7732-18-5) → ((N(CH2C5H4N)2CH2C5H3NN(CH2C6H5)2)Cu)2Cl2(2+)*2B(C6F5)4(1-)*4H2O=(((C32H31N5)Cu)2Cl2)(B(C6F5)4)2*4H2O

Guidance literature:

In tetrahydrofuran; under Ar; Cu complex dissolved in THF; CHCl3 added; pptd. by adding pentane; ppt. recrystd. from THF-pentane; elem. anal.;

DOI:10.1021/ic702437c

Reference yield:

Cu(1+)*(NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2*[B(C6F5)4](1-)=[Cu((NC5H4CH2)2NCH2C5H3NN(CH2C6H5)2)][B(C6F5)4] (1023595-89-2) + iodosylbenzene (536-80-1) → Cu(2+)*(NC5H4CH2)2NCH2C5H3NN(CH2C6H5)CH(O)C6H5(1-)=[Cu((NC5H4CH2)2NCH2C5H3NN(CH2C6H5)CH(O)C6H5)](1+)

Guidance literature:

In acetonitrile; a soln. of C6H5IO under Ar stirred for 30 min and cooled to -40°C, added anaerobically to a soln. of Cu complex at -40°C; not isolated, detected by MS;

DOI:10.1021/ic800617m

upstream raw materials:

tetrakis(acetonitrile)copper(I) tetrakis(pentafluorophenyl)borate

N(CH₂C₅H₄N)2CH₂C₅H₃NN(CH₂C₆H₅)2

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