trans-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

Base Information

Chemical Name:trans-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)
CAS No.:124751-48-0
Molecular Formula:C₃₄H₃₈Cl₂O₂P₂Pt
Molecular Weight:806.608
Hs Code.:

trans-((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C<sub>4</sub>H<sub>7</sub>O)2Cl<sub>2</sub>platinum(II)

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Chemical Property of trans-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

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Technology Process of trans-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

There total 5 articles about trans-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 41884-65-5,60479-35-8,51014-04-1
dichlorobis(trimethylacetonitrile)platinum(II)

: 91533-65-2
diphenyl(tetrahydro-2-furanylmethyl)phosphane

: 124751-48-0,124634-83-9
cis-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

Guidance literature:: In acetone; stirring (30 min); evapn.;
DOI:10.1039/DT9890002069

Reference yield: 85.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 91533-65-2
diphenyl(tetrahydro-2-furanylmethyl)phosphane

: 124751-48-0,124634-83-9
cis-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

Guidance literature:: In ethanol; water; exclusion of air, moisture; (Ar or N2); addn. of a soln. of K2PtCl4 in ethanol/water to a soln. of Ph2P(CH2)3CHCH2O in ethanol within 2 h; stirred for 20 h at room temp.; colorless precipitate; concn. of soln. in vac. to ca. 2/3 ; filtn.; washed with water, ethanol and ether; dried in high-vac.; elem. anal.;

Reference yield: 81.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 91533-65-2
diphenyl(tetrahydro-2-furanylmethyl)phosphane

: 124751-48-0,124634-83-9
cis-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

Guidance literature:: In dichloromethane; without air, moisture; (Ar or N2); addn. of Ph2P(CH2)3CHCH2O in CH2Cl2 to suspension of Cl2Pt(COD) in CH2Cl2 within 1 h at room temp.; stirred until a colorless soln. was formed; evapd. the volume of the react. mixture to ca. 5 ml; dissolved the residue in diethylether; stirring over night at 20°C; filtn.; washing with ethanol and ether; drying in high-vac.; elem. anal.;