C₁₈H₂₇NO₃Si

Base Information

Chemical Name:C₁₈H₂₇NO₃Si
CAS No.:1311407-00-7
Molecular Formula:C₁₈H₂₇NO₃Si
Molecular Weight:333.503
Hs Code.:

C<sub>18</sub>H<sub>27</sub>NO<sub>3</sub>Si

Synonyms:

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Chemical Property of C₁₈H₂₇NO₃Si

Chemical Property:

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Technology Process of C₁₈H₂₇NO₃Si

There total 6 articles about C₁₈H₂₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311406-98-0
C₁₂H₂₃NO₄Si

: 1311407-00-7
C₁₈H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 60 h / Reflux; Dean-Stark

With lithium borohydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jo2004617

Reference yield:

: 74844-91-0
1-tert-butyl 2-methyl (2S,4R)-4-hydroxy-1,2-pyrrolidinedicarboxylate

: 1311407-00-7
C₁₈H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: sodium periodate; ruthenium(IV) oxide / water; ethyl acetate

3: trifluoroacetic acid / dichloromethane / 5.33 h

4: lithium borohydride / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

5: toluene-4-sulfonic acid / toluene / 60 h / Reflux; Dean-Stark

With 1H-imidazole; ruthenium(IV) oxide; sodium periodate; lithium borohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo2004617

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1311407-00-7
C₁₈H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: sodium periodate; ruthenium(IV) oxide / water; ethyl acetate

3: trifluoroacetic acid / dichloromethane / 5.33 h

4: lithium borohydride / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

5: toluene-4-sulfonic acid / toluene / 60 h / Reflux; Dean-Stark

With 1H-imidazole; ruthenium(IV) oxide; sodium periodate; lithium borohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo2004617