N-Methyl-N-(4-methoxyphenyl)-4-nitrobenzamide

Base Information

• Chemical Name: N-Methyl-N-(4-methoxyphenyl)-4-nitrobenzamide
• CAS No.: 1092-52-0
• Molecular Formula: C₁₅H₁₄N₂O₄
• Molecular Weight: 286.287
• Hs Code.: 2924299090
• Mol file: 1092-52-0.mol

Synonyms:N-Methyl-N-p-nitrobenzoyl-p-methoxyanilin;p-Benzanisidide,N-methyl-4-nitro;Benzamide,N-(4-methoxyphenyl)-N-methyl-4-nitro;

Chemical Property of N-Methyl-N-(4-methoxyphenyl)-4-nitrobenzamide

Chemical Property:

• PSA: 75.36000
• LogP: 3.40320

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Methyl-N-(4-methoxyphenyl)-4-nitrobenzamide

There total 1 articles about N-Methyl-N-(4-methoxyphenyl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-methyl-N-(4-methoxyphenyl)amine (5961-59-1) + 4-nitro-benzoic acid (62-23-7) → N-(4-methoxyphenyl)-N-methyl-4-nitrobenzamide (1092-52-0)

Guidance literature:

With triethylamine; trichloromethyl chloroformate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1080/00304940509354888

Reference yield:

N-(4-methoxyphenyl)-N-methyl-4-nitrobenzamide (1092-52-0) → 6-methoxy-3-methyl-2-p-nitrophenylbenzoxazolium perchlorate

Guidance literature:

With sodium perchlorate; In methanol; at 0 ℃; electrolysis at 1.40 V;

DOI:10.1039/P29810001599

Reference yield:

N-(4-methoxyphenyl)-N-methyl-4-nitrobenzamide (1092-52-0) → 6-methoxy-3-methyl-2-p-nitrophenylbenzoxazolium perchlorate + N-methyl-4-nitrobenzamide (2585-23-1)

Guidance literature:

With sodium perchlorate; In methanol; at 0 ℃; Product distribution; electrolysis with/without added water;

DOI:10.1039/P29810001599

upstream raw materials:

N-methyl-N-(4-methoxyphenyl)amine

4-nitro-benzoic acid

Downstream raw materials:

N-methyl-4-nitrobenzamide

Refernces