Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl-

Base Information Edit

Chemical Name:Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl-
CAS No.:109276-10-0
Molecular Formula:C₁₃H₁₄O
Molecular Weight:186.254
Hs Code.:
NSC Number:167270
DSSTox Substance ID:DTXSID00304777
Mol file:109276-10-0.mol

Synonyms:Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl-;109276-10-0;NSC167270;SCHEMBL745582;DTXSID00304777;FKVIKTMLTIPULX-UHFFFAOYSA-N;NSC-167270;2-Phenylbicyclo[2.2.1]hept-5-en-2-ol;2-Phenylbicyclo[2.2.1]hept-5-en-2-ol #;2-Exo-phenylbicyclo[2.2.1]hept-5-en-2-ol

Suppliers and Price of Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl- Edit

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:186.104465066
Heavy Atom Count:14
Complexity:252

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2CC(C1C=C2)(C3=CC=CC=C3)O

Technology Process of Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl-

There total 9 articles about Bicyclo[2.2.1]hept-5-en-2-ol, 2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 694-98-4
norborn-5-en-2-one

: phenylmagnesium bromide

: 16187-25-0,57954-88-8,109276-10-0
2-phenylbicyclo<2.2.1>hept-5-en-2endo-ol

Guidance literature:: DOI:10.1016/S0040-4039(00)84955-2

Reference yield:

: 4,4,5,5-tetramethyl-2-(2-phenylbicyclo[2.2.1]hept-5-en-2-yl)-[1,3,2]-dioxaborolane

: 16187-25-0,57954-88-8,109276-10-0
endo-2-phenylbicyclo<2.2.1>hept-5-en-exo-2-ol

Guidance literature:: With dihydrogen peroxide; triethylamine; sodium hydroxide; In tetrahydrofuran; toluene; at 0 - 20 ℃; diastereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c4ra07415g

Reference yield:

: 4,4,5,5-tetramethyl-2-(2-phenylbicyclo[2.2.1]hept-5-en-2-yl)-[1,3,2]-dioxaborolane

: 16187-25-0,57954-88-8,109276-10-0
2-phenylbicyclo<2.2.1>hept-5-en-2endo-ol

: 16187-25-0,57954-88-8,109276-10-0
endo-2-phenylbicyclo<2.2.1>hept-5-en-exo-2-ol

Guidance literature:: With dihydrogen peroxide; triethylamine; sodium hydroxide; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 12h; Overall yield = 28.8 mg; diastereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c4ra07415g