Technology Process of C27H44BrNO2Si
There total 9 articles about C27H44BrNO2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja3121394
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 °C / Inert atmosphere
With
pyridine; triethylsilane; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja3121394
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere
2: 1H-imidazole; tert-butyldimethylsilyl chloride; dmap / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
3: pyridine / dichloromethane / 20 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
5: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 °C / Inert atmosphere
With
pyridine; 1H-imidazole; triethylsilane; dmap; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja3121394
