1-(p-formylphenylethynyl)-1'-iodoferrocene

Base Information

Chemical Name:1-(p-formylphenylethynyl)-1'-iodoferrocene
CAS No.:72022-49-2
Molecular Formula:C₁₉H₁₃FeIO
Molecular Weight:440.063
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(p-formylphenylethynyl)-1'-iodoferrocene

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Technology Process of 1-(p-formylphenylethynyl)-1'-iodoferrocene

There total 1 articles about 1-(p-formylphenylethynyl)-1'-iodoferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 12145-93-6
1,1'-diiodoferrocene

: 72034-29-8
p-ethynylbenzaldehyde diethyl ether acetal

: 72022-49-2
1-(p-formylphenylethynyl)-1'-iodoferrocene

: 72022-48-1
1,1'-bis(p-formylphenylethynyl)ferrocene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In diethylamine; High Pressure; mixt. of complex, HC2C6H4CH(OC2H5)2, CuI, (Ph3P)2PdCl2 and (C2H5)3N heated under N2 in autoclave at 80°C for 8 h; (C2H5)3N removed (vac.), CHCl3 and H2O added, CHCl3 layer washed with aq. HCl, washed with satd. NaHCO3 soln. and satd. NaCl soln., dried (MgSO4), filtered, concd., chromd. (SiO2, C6H6/CHCl3); elem. anal.;
DOI:10.1246/bcsj.56.1143