isonicotinyl hydrazine

Base Information

• Chemical Name: isonicotinyl hydrazine
• CAS No.: 1303186-77-7
• Molecular Formula: C₂₀H₁₆N₆O₂
• Molecular Weight: 372.386
• Mol file: 1303186-77-7.mol

Synonyms:

Chemical Property of isonicotinyl hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of isonicotinyl hydrazine

There total 2 articles about isonicotinyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

picolinic acid hydrazide (1452-63-7) + Isophthalaldehyde (626-19-7) → isonicotinyl hydrazine (1303186-77-7)

Guidance literature:

In ethanol; for 4h; Reflux;

DOI:10.1039/c4ob00653d

Reference yield:

2-Picolinic acid (98-98-6) → isonicotinyl hydrazine (1303186-77-7)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / 1.5 h / Reflux

2: hydrazine hydrate / Reflux

3: ethanol / 4 h / Reflux

With thionyl chloride; hydrazine hydrate; In ethanol;

DOI:10.1039/c4ob00653d

upstream raw materials:

2-Picolinic acid

picolinic acid hydrazide

Isophthalaldehyde