trimethylsilylphenyldiethylgermane

Base Information

Chemical Name:trimethylsilylphenyldiethylgermane
CAS No.:104585-85-5
Molecular Formula:C₁₃H₂₄GeSi
Molecular Weight:281.009
Hs Code.:

Synonyms:

Suppliers and Price of trimethylsilylphenyldiethylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethylsilylphenyldiethylgermane

Chemical Property:

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Technology Process of trimethylsilylphenyldiethylgermane

There total 3 articles about trimethylsilylphenyldiethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 100471-86-1
bis(trimethylsilyldiethylgermyl)mercury

: 104585-85-5
trimethylsilylphenyldiethylgermane

Guidance literature:: With bromobenzene; lithium; In hexane; Hg-comp. and Li stirred at 20°C for 24 h, filtered, halide added, at -78°C stirred for 1 h; heated to 20°C; elem. anal.;

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 6727-87-3
triethylgermyllithium

: 79301-90-9
phenyldiethylgermane

: 104585-85-5
trimethylsilylphenyldiethylgermane

: 1188-14-3
Triethylgerman

: 7749-85-1
trimethylsilyltriethylgermane

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; Metallation of PhEt2GeH with Et3GeLi in HMPA is followed by addn. of excess Me3SiCl.;
DOI:10.1016/0022-328X(81)80004-6

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 112520-68-0
phenyldiethylgermyllithium

: 79301-90-9
phenyldiethylgermane

: 104585-85-5
trimethylsilylphenyldiethylgermane

Guidance literature:: With methanol; water; In tetrahydrofuran; hexane; benzene; vac.; addn. of MeOH in THF/benzene to Ge-compound in THF (-78°C), after 5 min addn. of Me3SiCl, stirring (room temp., 1 h), addn. of water and hexane; sepn. of org. layer, drying (MgSO4); GLC anal.; Kinetics;