1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene

Base Information

Chemical Name:1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene
CAS No.:871732-70-6
Molecular Formula:C₄₀H₅₁BrFeO
Molecular Weight:683.595
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene

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Technology Process of 1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene

There total 1 articles about 1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 284688-05-7
1-(4'-bromobiphenyl-4-yl)-ferrocene

: 112-76-5
Stearoyl chloride

: 871732-70-6
1-(4'-bromobiphenyl-4-yl)-1'-n-stearoylferrocene

Guidance literature:: With AlCl₃; In carbon disulfide; at 20°C under Ar atm.; mixt. of AlCl3, CS2 and C17H35COCl stirredfor 2.5 h, then soln. of Fe-complex added (ratio Fe-complex:C17H35COCl: AlCl3=1.0:1.0:1.6), stirred for 2.5 h, poured onto ice, concd. HCl and CHCl3 added; org. layer septd., washed (water), dried (MgSO4), filtered, solvent removed in vacuo, residue chromatographed on Al2O3, eluted with 2:1 C6H6:light petroleum, twice recrystd. from light petroleum; elem. anal.;
DOI:10.1007/s11172-005-0053-6