[⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

Base Information

Chemical Name:[⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]
CAS No.:126285-66-3
Molecular Formula:C₄₄H₂₈ClFeN₄
Molecular Weight:705.186
Hs Code.:

[<sup>(57)</sup>Fe(tetraphenylporphyrin)Cl]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

Chemical Property:

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Technology Process of [⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

There total 2 articles about [⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: ferrous-57 acetate

: 126285-66-3
[⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

Guidance literature:: With oxygen; sodium chloride; In hydrogenchloride; dichloromethane; under Ar, (57)Fe-acetate soln. in AcOH:Ac2O was added to soln. of porphyrine-compd. and NaCl in CH2Cl2, mixt. was refluxed and Ar was replaced with O2, 1 h; solvent was removed, concd. HCl was added, stirring for 1 h; solvent was removed, residue was dissolved in CHCl3, hot MeOH was added,cooling, crystals were filtered off, dried at 125 °C/2 Torr;
DOI:10.1021/jp0266087

Reference yield:

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: ⁽⁵⁷⁾iron(II) chloride

: 126285-66-3
[⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

Guidance literature:: DOI:10.1021/ja801860u

Reference yield:

: 126285-66-3
[⁽⁵⁷⁾Fe(tetraphenylporphyrin)Cl]

: 594-09-2
trimethylphosphane

: {(C₆H₅)4C₂₀H₈N₄⁽⁵⁷⁾Fe(P(CH₃)3)2}

Guidance literature:: With zinc amalgam; In benzene-d6; toluene; (Ar); reduction of Fe(III) porphyrin complex with zinc amalgam in C6D6, stirring (2 h), titration by PMe3 in toluene;
DOI:10.1021/ja00141a027