bis(p-dimethylsilylphenyl)dimethylstannane

Base Information

Chemical Name:bis(p-dimethylsilylphenyl)dimethylstannane
CAS No.:861857-11-6
Molecular Formula:C₁₈H₂₈Si₂Sn
Molecular Weight:419.301
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(p-dimethylsilylphenyl)dimethylstannane

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Technology Process of bis(p-dimethylsilylphenyl)dimethylstannane

There total 1 articles about bis(p-dimethylsilylphenyl)dimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1637-65-6
4-dimethylsilylphenylmagnesium bromide

: 753-73-1
dimethyltin dichloride

: 861857-11-6
bis(p-dimethylsilylphenyl)dimethylstannane

Guidance literature:: With Mg; In tetrahydrofuran; treatment of p-bromophenyldimethylsilane with Mg turnings in THF; slow addn. of soln. of SnCl2Me2 in THF; reflux for 12 h; pouring into ice water, extn. with ether, drying of combined org. extracts over Na2SO4; removal of volatiles under reduced pressure, purification by Kugelrohr distn.; as oil; elem. anal.;
DOI:10.1021/om050265s

Reference yield: 53.0%

: 861857-11-6
bis(p-dimethylsilylphenyl)dimethylstannane

: 7732-18-5
water

: 861857-14-9
bis(p-dimethylhydroxysilylphenyl)dimethylstannane

Guidance literature:: With Pd(OH)2/C; In tetrahydrofuran; water; byproducts: H2; slow addn. of soln. of p,p'-HMe2SiC6H4SnMe2C6H4SiMe2H in THF to ice-coldsuspn. of Pearlman's catalyst in THF and H2O; evolution of H2; stirring at room temp. for 15 min; filtration, removal of solvent at 30°C under reduced pressure, addn. of ether; removal of aq. layer; drying over Na2SO4; addn. of hexane;concn. under reduced pressure at 30°C; pptn. at -10°C; el em. anal.;
DOI:10.1021/om050265s