4,5-diphenyl-3-ethylisoxazole

Base Information

Chemical Name:4,5-diphenyl-3-ethylisoxazole
CAS No.:181696-91-3
Molecular Formula:C₁₇H₁₅NO
Molecular Weight:249.312
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-diphenyl-3-ethylisoxazole

Chemical Property:

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Technology Process of 4,5-diphenyl-3-ethylisoxazole

There total 4 articles about 4,5-diphenyl-3-ethylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16737-10-3
1,2-diphenyl-1-pentene-3-one oxime

: 181696-91-3
4,5-diphenyl-3-ethylisoxazole

Guidance literature:: With iodine; sodium hydrogencarbonate; potassium iodide; In tetrahydrofuran; water; for 5h; Heating / reflux;

Reference yield:

: 1007-32-5
benzyl ethyl ketone

: 181696-91-3
4,5-diphenyl-3-ethylisoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / acetic acid / 20 h / 0 - 20 °C

2: potassium hydroxide; hydroxylamine hydrochloride / ethanol; water / 3.5 h / 75 °C / Heating / reflux

3: iodine; sodium hydrogencarbonate; potassium iodide / tetrahydrofuran; water / 5 h / Heating / reflux

With potassium hydroxide; hydroxylamine hydrochloride; hydrogen bromide; iodine; sodium hydrogencarbonate; potassium iodide; In tetrahydrofuran; ethanol; water; acetic acid;

Reference yield:

: 16736-09-7
1,2-diphenylpent-1-en-3-one

: 181696-91-3
4,5-diphenyl-3-ethylisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; hydroxylamine hydrochloride / ethanol; water / 3.5 h / 75 °C / Heating / reflux

2: iodine; sodium hydrogencarbonate; potassium iodide / tetrahydrofuran; water / 5 h / Heating / reflux

With potassium hydroxide; hydroxylamine hydrochloride; iodine; sodium hydrogencarbonate; potassium iodide; In tetrahydrofuran; ethanol; water;