dimesitylstibane

Base Information

Chemical Name:dimesitylstibane
CAS No.:121810-02-4
Molecular Formula:C₁₈H₂₃Sb
Molecular Weight:361.131
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimesitylstibane

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Technology Process of dimesitylstibane

There total 3 articles about dimesitylstibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: CpCp(*)Hf(SbMes₂)2

: 121810-02-4
dimesitylstibane

: (η5-C5H5)(η5-C5Me5)Cl2hafnium

Guidance literature:: In diethyl ether; Hf complex reacted with ethereal HCl; crystd. fractionally from hexane;
DOI:10.1021/ic061826q

Reference yield: 68.0%

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

: 121810-02-4
dimesitylstibane

Guidance literature:: With Li; NH(CH₃)3Cl; In tetrahydrofuran; toluene; stirring of a soln. of Sb compd. and Li in THF for 12 h at 25°C, filtration, treatment with solid NHMe3Cl, stirring for 2 h, soln. was concd., treated with toluene, filtered and solvent removed in vac.; recrystn. from toluene/hexane (3:1) at -15°C;

Reference yield:

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

: ammonium chloride

: 121810-02-4
dimesitylstibane

Guidance literature:: With lithium; Mes3Sb reacted with excess Li wire, followed by the protonation of the formed antimonide with NH4Cl in according with method of Cowley et al. (Angew. Chem. 101 (1989) 1089-1090);
DOI:10.1016/j.jorganchem.2010.09.007