Mes₂SPCH₂CH₂B(C₆F₅)2

Base Information

Chemical Name:Mes₂SPCH₂CH₂B(C₆F₅)2
CAS No.:1403338-71-5
Molecular Formula:C₃₂H₂₆BF₁₀PS
Molecular Weight:674.393
Hs Code.:

Mes<sub>2</sub>SPCH<sub>2</sub>CH<sub>2</sub>B(C<sub>6</sub>F<sub>5</sub>)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mes₂SPCH₂CH₂B(C₆F₅)2

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Technology Process of Mes₂SPCH₂CH₂B(C₆F₅)2

There total 2 articles about Mes₂SPCH₂CH₂B(C₆F₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1003010-54-5
dimesitylvinylphosphine

: 7704-34-9
sulfur

: 165612-94-2
bis(pentafluorophenyl)borohydride

: 1403338-71-5
Mes₂SPCH₂CH₂B(C₆F₅)2

Guidance literature:: In benzene; mixt. of phosphane and borane dissolved in pentane, stirred for 10 min; S added; stirred for 3 d; volatiles removed in vacuo; resdiue dried in vacuo; crystd. from D6-benzene at room temp.; elem. anal.;
DOI:10.1002/ejic.201200288

Reference yield:

: 7719-09-7
thionyl chloride

: 1003010-54-5
dimesitylvinylphosphine

: 165612-94-2
bis(pentafluorophenyl)borohydride

: 1403338-70-4
Mes₂OPCH₂CH₂B(C₆F₅)2

: 1403338-68-0
Mes₂ClPCH₂CH₂BCl(C₆F₅)2

: 1403338-71-5
Mes₂SPCH₂CH₂B(C₆F₅)2

Guidance literature:: In benzene-d6; mixt. of phosphane and borane dissolved in D6-benzene, stirred; SOCl2 added; stirred for 90 min; detd. by (19)F NMR;
DOI:10.1002/ejic.201200288