dimesitylvinylphosphine

Base Information

• Chemical Name: dimesitylvinylphosphine
• CAS No.: 1003010-54-5
• Molecular Formula: C₂₀H₂₅P
• Molecular Weight: 296.392
• Mol file: 1003010-54-5.mol

Synonyms:dimesitylvinylphosphine

Chemical Property of dimesitylvinylphosphine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of dimesitylvinylphosphine

There total 2 articles about dimesitylvinylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

bis(2,4,6-trimethylphenyl)chlorophosphine (67950-05-4) + vinyl magnesium bromide (1826-67-1) → dimesitylvinylphosphine (1003010-54-5)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1039/b710475h

Reference yield:

((CH3)3C6H2)2PCH2CH2B(C6F5)2(CO2) → dimesitylvinylphosphine (1003010-54-5)

Guidance literature:

In dichloromethane; byproducts: CO2; >-20°C;

DOI:10.1002/anie.200901636

Reference yield: 90.0%

dimesitylvinylphosphine (1003010-54-5) + C16H8BF12(1-)*2C4H10O*Li(1+) → C36H32BF12P

Guidance literature:

With chloro-trimethyl-silane; In pentane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.201601583

upstream raw materials:

bis(2,4,6-trimethylphenyl)chlorophosphine

vinyl magnesium bromide

Downstream raw materials:

Ph₂P-C₂H₄-B(C₆F₅)2

[2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

C₃₇H₃₃BF₁₀P^(1-)*H⁽¹⁺⁾