(2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

Base Information

Chemical Name:(2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2
CAS No.:107474-16-8
Molecular Formula:C₆₀H₈₅N₅O₂Re₂
Molecular Weight:1280.78
Hs Code.:

(2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>N)3ReORe(O)(N-2,6-C<sub>6</sub>H<sub>3</sub>iPr<sub>2</sub>)2

Synonyms:

Suppliers and Price of (2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

There total 2 articles about (2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 2008-61-9
2,6-diisopropylphenylisocyanide

: 16687-12-0
trimethylsilylperrhenate

: 118968-24-4
Re(N(2,6-diisopropylphenyl)3)(OSiMe₃)

: 107474-16-8
(2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

: 118968-27-7
Re(O)(N-2,6-C₆H₃iPr₂)2(OSiMe₃)

Guidance literature:: In further solvent(s); solvent: (Me3Si)2O, refluxed for 18 h; removal of solvent in vac., extn. (pentane), left behind Re2O2(NAr)5, extract concd., cooled, recrystn. (-30°C/pentane); elem. anal.;
DOI:10.1016/S0277-5387(00)80695-6

Reference yield: 30.0%

: 28178-42-9
2,6-diisopropylphenyl isocyanate

: 16687-12-0
trimethylsilylperrhenate

: 2Re⁽⁷⁺⁾*3O^(2-)*4((CH₃)2CH)2C₆H₃N^(2-)=Re₂O₃(NC₆H₃(CH(CH₃)2)2)4

: 107474-16-8
(2,6-iPr₂C₆H₃N)3ReORe(O)(N-2,6-C₆H₃iPr₂)2

Guidance literature:: In toluene; ReO3(OSiMe)3 was treated with 3 equiv of ArNCO in refluxing toluene for 5 h; at least one more unidentified product was formed; identification on the basis of elem. anal. and (1)H NMR spectral data;
DOI:10.1021/om00147a038