bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel

Base Information

Chemical Name:bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel
CAS No.:957319-65-2
Molecular Formula:C₅₄H₇₄N₄NiO₂
Molecular Weight:869.897
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel

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Technology Process of bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel

There total 1 articles about bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 110-86-1
pyridine

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: potassium N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidate

: 98-88-4
benzoyl chloride

: [N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel(pyridine)

: 957319-65-2
bis[N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2N,O](η1-benzoyl)nickel

Guidance literature:: In tetrahydrofuran; (inert atm., dark); addn. of benzoyl chloride and pyridine in THF to soln. of nickel compd. in THF at room temp., keeping for 15 min, addn. of THF soln. of potassium salt over 45 min, stirring overnight; evapn., extn. (ether), filtration, concg., keeping at room temp. overnight, isolation of crystals, recrystn. (pentane-ether), NMR;
DOI:10.1021/om070155g