Technology Process of C40H53N5O11Si
There total 8 articles about C40H53N5O11Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C39H49N5O11Si;
With
sodium cyanoborohydride; acetic acid;
at 5 - 20 ℃;
for 1.25h;
formaldehyd;
With
sodium cyanoborohydride;
In
water;
at 5 - 20 ℃;
for 1.25h;
DOI:10.1081/NCN-120028337
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 86 percent / (N,N-dimethylamino)pyridine / acetonitrile / 20 °C
2.1: 45 percent / AIBN / benzene / Heating
3.1: NaIO4; OsO4 / H2O / 5 h / 20 °C
4.1: acetic acid / CH2Cl2; toluene / 35 °C / atmospheric pressure
5.1: 0.17 g / Cl3CCO2H / CH2Cl2 / 0.17 h / 20 °C
6.1: sodium cyanoborohydride; glacial acetic acid / 1.25 h / 5 - 20 °C
6.2: sodium cyanoborohydride / H2O / 1.25 h / 5 - 20 °C
With
dmap; sodium periodate; osmium(VIII) oxide; 2,2'-azobis(isobutyronitrile); sodium cyanoborohydride; acetic acid; trichloroacetic acid;
In
dichloromethane; water; toluene; acetonitrile; benzene;
DOI:10.1081/NCN-120028337
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 92.6 percent / imidazole / dimethylformamide / 12 h / 20 °C
2.1: 79 percent / methylhydrazine / CH2Cl2 / 1 h / 0 °C
3.1: acetic acid / CH2Cl2; toluene / 35 °C / atmospheric pressure
4.1: 0.17 g / Cl3CCO2H / CH2Cl2 / 0.17 h / 20 °C
5.1: sodium cyanoborohydride; glacial acetic acid / 1.25 h / 5 - 20 °C
5.2: sodium cyanoborohydride / H2O / 1.25 h / 5 - 20 °C
With
1H-imidazole; sodium cyanoborohydride; acetic acid; methylhydrazine; trichloroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1081/NCN-120028337
