1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride

Base Information

Chemical Name:1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride
CAS No.:1192011-03-2
Molecular Formula:C₂₂H₁₉N₄*Cl
Molecular Weight:374.873
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride

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Technology Process of 1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride

There total 1 articles about 1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 4857-04-9
2-chloromethyl-1H-benzimidazole

: 4981-92-4
1-benzylbenzimidazole

: 1192011-03-2
1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride

Guidance literature:: In 1,4-dioxane; at 100 ℃; for 48h; Inert atmosphere;
DOI:10.1039/b905036a

Reference yield: 61.0%

: 67-66-3,8013-54-5
chloroform

: 1192011-03-2
1-(benzimidazol-2-ylmethyl)-3-benzylbenzimidazolium chloride

: 83864-14-6
nickel dichloride

: bis(1-(benzimidazolato-2-ylmethyl)-3-benzylbenzimidazol-2-ylidene)nickel(II)*0.25(chloroform)

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; under Ar; mixt. of imidazolium salt, dry NiCl2 and K2CO3 heated in DMF at 130°C for 16 h; cooled; filtered; filtrate evapd. to dryness in vac.; dissolved in CH2Cl2; washed with H2O and brine; dried (MgSO4); solvent reduced in vol.; Et2O added; filtered; ppt. washed with Et2O; dried in vac.; recrystd. from CHCl3-Et2O; elem. anal;
DOI:10.1039/b905036a