C₂₄H₄₄NO₈⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₂₄H₄₄NO₈⁽¹⁺⁾*Br^(1-)
• CAS No.: 1482517-83-8
• Molecular Formula: Br*C₂₄H₄₄NO₈
• Molecular Weight: 554.519
• Mol file: 1482517-83-8.mol

Synonyms:

Chemical Property of C₂₄H₄₄NO₈⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₄₄NO₈⁽¹⁺⁾*Br^(1-)

There total 7 articles about C₂₄H₄₄NO₈⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzylbromide (246140-08-9) + trimethylamine (75-50-3) → C24H44NO8(1+)*Br(1-) (1482517-83-8)

Guidance literature:

In ethanol; at 80 ℃; for 24h;

DOI:10.1002/chem.201300289

Reference yield:

triethylene glucol monomethyl ether (112-35-6,95507-80-5) → C24H44NO8(1+)*Br(1-) (1482517-83-8)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium hydroxide / water; tetrahydrofuran / 34 h / 20 °C / Cooling

2: potassium carbonate; 18-crown-6 ether / acetone / 24 h / 70 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 15 h / 5 - 25 °C

4: phosphorus tribromide / benzene / 6 h / 20 °C / Cooling with ice

5: ethanol / 24 h / 80 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; phosphorus tribromide; potassium carbonate; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetone; benzene;

DOI:10.1002/chem.201300289

Reference yield:

(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-phenyl)-methanol (206049-37-8) → C24H44NO8(1+)*Br(1-) (1482517-83-8)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus tribromide / benzene / 6 h / 20 °C / Cooling with ice

2: ethanol / 24 h / 80 °C

With phosphorus tribromide; In ethanol; benzene;

DOI:10.1002/chem.201300289

upstream raw materials:

3,5-Dihydroxybenzoic acid

triethylene glucol monomethyl ether

1-carbomethoxy-3,5-dihydroxybenzene

3,5-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzylbromide